Agricola, Georgius, De re metallica, 1912/1950

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If to the first aqua the other which contains silver is to be added, it
must
be poured in before the powerful vapours appear, and the aqua gives off
the
oily substance, and the operculum becomes red; for he who pours in the
aqua after the vapour appears causes a loss, because the aqua generally spurts
out
and the glass breaks.
If the ampulla breaks when the gold is being parted
from
the silver or the silver from the aqua, the aqua will be absorbed by the
sand
or the lute or the bricks, whereupon, without any delay, the red hot coals
should
be taken out of the furnace and the fire extinguished.
The sand and
bricks
after being crushed should be thrown into a copper vessel, warm water.
should be poured over them, and they should be put aside for the space of
twelve
hours; afterward the water should be strained through a canvas, and
the
canvas, since it contains silver, should be dried by the heat of the sun or
the
fire, and then placed in an earthen crucible and heated until the silver
melts
, this being poured out into an iron mould.
The strained water should
be
poured into an ampulla and separated from the silver, of which it contains
a
minute portion; the sand should be mixed with litharge, glass-galls,
argol
, saltpetre, and salt, and heated in an earthen crucible.
The button
which
settles at the bottom should be transferred to a cupel, and should
be
re-melted, in order that the lead may be separated from the silver.
The
lute
, with lead added, should be heated in an earthen crucible, then
re-melted
in a cupel.

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